Synthesis, Characterization and Thermal Analysis   (TGA and DSC) of Novel Schiff Base Derivatives From 4-Chloro-2-Fluoro aniline and its Complexes with Copper (II) and Nickel (II) Ions

Authors

  • Haneen Shaker Sachit Department of Chemistry, College of Science, University of Thi-Qar, Iraq
  • Haider Abbas Mahdi Department of Chemistry, College of Science, University of Thi-Qar, Iraq

Keywords:

Schiff bases, 4-Chloro-2-fluoroaniline, 3-Ethoxysalicyldehyde, Copper(II) complex, 4-Methoxysalicyldehyde, Nickel(II) complex

Abstract

Preparation of Schiff Bases from the Reaction of 4-Chloro-2-fluoroaniline with 3-Ethoxysalicyldehyde (Ligand 1) and 4-Methoxysalicyldehyde (Ligand 2) and Their Complexation with Copper(II) Chloride (1:2) and Nickel(II) Chloride (1:1). characterization on the basis their spectra of 1H-NMR, Fourier transform infrared (FTIR), and Differential scanning calorimetry to assess the thermal characteristics of the produced  (DSC). Elemental analysis and spectral data of the ligands were found to be in a good agreement with their structures, and their complexes with Cu (II) and Ni (II) were synthesized.

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Published

2025-11-10

How to Cite

Synthesis, Characterization and Thermal Analysis   (TGA and DSC) of Novel Schiff Base Derivatives From 4-Chloro-2-Fluoro aniline and its Complexes with Copper (II) and Nickel (II) Ions. (2025). Information Horizons: American Journal of Library and Information Science Innovation (2993-2777), 3(11), 42-57. https://www.grnjournal.us.e-scholar.org/index.php/AJLISI/article/view/8479